Development of novel microsphere structured – calcium tungstate as efficacious electrocatalyst for the detection of antibiotic drug nitrofurantoin

文献情報

出版日 2023-11-20

DOI 10.1039/D3TB02087H

インパクトファクター 6.331

著者

P. Manikanta, Mounesh, Rohit Rangnath Nikam, S. Sandeep, Bhari Mallanna Nagaraja

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要旨

In this report, synthetic and nitro groups containing antibiotic drug nitrofurantoin (NFT) were electrochemically quantified under amended conditions using novel constructed calcium tungstate microspheres modified on glassy carbon electrodes (CTMs/GCE). The calcium tungstate microspheres (CTMs) were synthesized by a facile sonochemical method and characterizations were done by various techniques, such as X-ray diffraction spectrometry (XRD), Fourier transform infrared spectroscopy (FTIR), Raman, field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy (XPS), and transmission electron microscopy (TEM). Ahead of this, electrochemical investigations were performed using electrochemical impedance spectroscopy (EIS), cyclic voltammetry (CV), amperometry, and linear sweep voltammetry (LSV). The synthesis of CTMs as well-distributed microspheres allows more active metal sites regarding and remarkable electrocatalytic activity towards NFT detection with excellent sensitivity (0.724 μA μM−1 cm−2) and low detection limit (21 nmol L−1) with a wide linear range 10–140 μM. The practical feasibility of the developed CTMs/GC electrode was elucidated using distinct real sample river tap water and clinical sample (NFT capsule), and thus, the modified electrode manifested acceptable recovery results.

掲載誌

Journal of Materials Chemistry B

CiteScore: 12

自己引用率: 4.9%

年間論文数: 831

Journal of Materials Chemistry A, B & C cover high quality studies across all fields of materials chemistry. The journals focus on those theoretical or experimental studies that report new understanding, applications, properties and synthesis of materials. The journals have a strong history of publishing quality reports of interest to interdisciplinary communities and providing an efficient and rigorous service through peer review and publication. The journals are led by an international team of Editors-in-Chief and Associate Editors who are all active researchers in their fields. Journal of Materials Chemistry A, B & C are separated by the intended application of the material studied. Broadly, applications in energy and sustainability are of interest to Journal of Materials Chemistry A, applications in biology and medicine are of interest to Journal of Materials Chemistry B, and applications in optical, magnetic and electronic devices are of interest to Journal of Materials Chemistry C. More than one Journal of Materials Chemistry journal may be suitable for certain fields and researchers are encouraged to submit their paper to the journal that they feel best fits for their particular article. Example topic areas within the scope of Journal of Materials Chemistry B are listed below. This list is neither exhaustive nor exclusive. Antifouling coatings Biocompatible materials Bioelectronics Bioimaging Biomimetics Biomineralisation Bionics Biosensors Diagnostics Drug delivery Gene delivery Immunobiology Nanomedicine Regenerative medicine & Tissue engineering Scaffolds Soft robotics Stem cells Therapeutic devices image block All articles published in Journal of Materials Chemistry B from 2019 onwards will be indexed in MEDLINE®. Articles that primarily focus on providing insight into the underlying science and performance of biomaterials within a biological environment are more suited to our companion journal, Biomaterials Science.

Development of novel microsphere structured – calcium tungstate as efficacious electrocatalyst for the detection of antibiotic drug nitrofurantoin

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