Synthesis of carbamates from amines and N-tosylhydrazones under atmospheric pressure of carbon dioxide without an external base

文献情報

出版日 2016-04-19

DOI 10.1039/C6QO00111D

インパクトファクター 5.281

著者

Ji Young Hong, Ue Ryung Seo, Young Keun Chung

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要旨

The methodology for the synthesis of carbamates via the base-promoted coupling of carbon dioxide, amines, and N-tosylhydrazones using potassium carbonate as the base and the pressure of 4 MPa of carbon dioxide has been published by Jiang et al. (2015). We demonstrated that this method provides the desired carbamates under just 1 atm of carbon dioxide without the addition of a base promoter. Thus, carbamates were successfully synthesized under mild reaction conditions in moderate to high yields.

掲載誌

Organic Chemistry Frontiers

CiteScore: 7.8

自己引用率: 8.7%

年間論文数: 724

Organic Chemistry Frontiers publishes high-quality research from across organic chemistry. Emphases are placed on studies that make significant contributions to the field of organic chemistry by reporting either new or significantly improved protocols or methodologies. Topics include, but are not limited to the following: Organic synthesis Development of synthetic methodologies Catalysis Natural products Functional organic materials Supramolecular and macromolecular chemistry Physical and computational organic chemistry

Synthesis of carbamates from amines and N-tosylhydrazones under atmospheric pressure of carbon dioxide without an external base

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