Quantitative determination of lead in mixtures of lead(ii) halides using solid-state 207Pb NMR spectroscopy

文献情報

出版日 2006-09-05

DOI 10.1039/B609870C

インパクトファクター 4.616

著者

Alicia Glatfelter, Nicole Stephenson, Shi Bai, Cecil Dybowski, Dale L. Perry

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要旨

We demonstrate a multi-spectrum technique for facile, quantitative determination of lead in solid materials using solid-state 207Pb NMR that avoids the major problem of uniform excitation across a wide spectral range; the method can be employed without chemical separation or other chemical manipulations and without any prior sample preparation, resulting in a non-destructive analysis, and producing results that are in agreement with gravimetric analyses of mixed samples of the lead halides.

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CiteScore: 7.8

自己引用率: 5.6%

年間論文数: 653

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Quantitative determination of lead in mixtures of lead(ii) halides using solid-state 207Pb NMR spectroscopy

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